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I can now sync with HotSync (but of course, all my "events" and contacts are with iCal and Address Book. When I try to enable iSync, I find that I cannot add my device! On checking things in System Profiler, my Treo does NOT show up in the USB list, yet, as I said, I can sync via USB.
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Before this started, did you add anything new or change something that would have caused this?
Try restarting with your Tiger CD and "repairing permissions". If you haven't done this before, it's very easy. You launch Disk Utility prior to installation and you can select Repair Permissions. Hope this is clear. Given all the steps you taken with installing/uninstalling, I'm guessing that you're a Mac pro.
Also, check out this thread
Cannot Enable Palm OS Syncing.
Hope this helps.
-Chris